DAROU PAKHSH PHARMA. CHEM . Co.

DAROU PAKHSH PHARMA.CHEM. CO.

Quality control Lab

Certificate of analysis

   Product:    Mebendazole           C16H13N3O3

Test

Limits

Description

A white TO slightly yellow powder. It shows polymorphism.

Solubility

Practically insoluble in water, in alcohol, in ether and in methylene chloride.

Identification

A. UV absorption maximum, at 247 nm and 312 nm, the specific absorbances at these maximum are 940 to 1040 and 485 to 535, respectively. B. Infrared spectrophotometry as same as Mebendazol CRS. C. An intense yellow color is produced.

Related substances TLC

Any other spot other than main spot not more intensely than 0.25% and the sum spot other than main spot not more than 0.5%.

Heavy metals

Not more than 20 ppm.

Loss on drying

Not more than 0.5 percent

Sulphated ash

Not more than 0.1 percent.

ASSAY

98.0 - 102.0 % w/w calculated with reference to the dried substance.

This material has been prepared following the good manufacturing practice (G.M.P.) and conforms above specification & requirements of BP2000